Isolation and extraction of lucidin primeveroside from Rubia tinctorum L. and crystal structure elucidation

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Isolation and extraction of lucidin primeveroside from Rubia tinctorum L. and crystal structure elucidation.

Madder (Rubia tinctorum L.) has been used as a dye for over 2000 years with alizarin and purpurin the major natural dyes analysed from extractions undertaken. The use of ethanol as the solvent in the extraction process produced an extract that yielded four anthraquinone compounds lucidin primeveroside, ruberythric acid, alizarin and lucidin-ω-ethyl ether. Gravitational separation of the extract...

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Isolation and extraction of ruberythric acid from Rubia tinctorum L. and crystal structure elucidation.

Madder (Rubia tinctorum L.) has been exploited as a dye throughout history. The roots of the plant are very rich in the highly coloured glycosidic compounds ruberythric acid and lucidin primeveroside, alongside the corresponding aglycons which can be readily formed by deglycosylation, particularly during extraction. Supported by (1)H and (13)C NMR data, the conclusive X-ray crystal structure of...

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extraction and acetylation of purified trypsin from bovin pancreas and study of some its physico-chemical properties

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15 صفحه اول

A multivariate study of the performance of an ultrasound-assisted madder dyes extraction and characterization by liquid chromatography-photodiode array detection.

An extraction method of madder (Rubia tinctorum) roots dyes is established and optimized to obtain the original chemical composition. A central composite design (CCD) was developed to specify the importance of the three major factors studied (time, temperature and solvent composition) affecting the ultrasound-assisted extraction of this matrix. A preliminary granulometric study of madder roots ...

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Isolation and structure elucidation of coumarin and cinamate derivatives from Lycium ruthenicum

Lycium species is a popular medicinal plant in the traditional Chinese medicine and Lycium ruthenicum is a native medicinal plant of Iran. Lycium genus has several biologically important properties too. Investigation of chemical composition of ethyl acetate extract of this plant is the goal of this study. Two coumarins (Scopoletin and Sculetin) and Methyl-2-hydroxy-4-undecanoxy-trans-cinamate w...

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ژورنال

عنوان ژورنال: Phytochemistry

سال: 2013

ISSN: 0031-9422

DOI: 10.1016/j.phytochem.2013.07.001